The fiber/matrix interaction of high modulus (M40) and intermediate mo
dulus (T800) carbon fibers with a bismaleimide resin has been studied
by means of three micromechanical techniques involving a single fiber,
namely, fragmentation, Raman spectroscopy, and pullout. A number of c
hemical treatments aimed at improving the fiber/matrix stress transfer
at elevated temperature were tested. The stress transfer proved to be
reduced by the temperature in the same way for all interfacial condit
ions. The limitations to the micromechanical characterization of model
composites in temperature are emphasized.