N. Kaltenkirchen et al., MECHANICAL-PROPERTIES OF NEW LOW-VISCOSIT Y POLYMETHYL METHACRYLATE BONE CEMENTS - IMPROVEMENT THROUGH VACUUM-MIXING, Der Unfallchirurg, 99(7), 1996, pp. 492-497
With the objective of improving mechanical properties by using a new c
atalyst, a new bone cement (Sulfix-60) and a new low-viscosity cement
with added gentamycin (Allofix-G) were developed. Dynamic weakness was
the major disadvantage of the older Sulfix-6 cement, especially in co
mparison with high-viscosity bone cement. Although static strength cou
ld be improved, investigations into improved fatigue strength and the
effect of vaccuum-mixing on the static and fatigue strength had yet to
be carried out. To investigate fatigue stability, specimens of the ne
w bone cements were tested using loads under wet conditions until brea
kage or 20 million cycles. In a first series the cement was hand-mixed
, in a second series vacuum-mixed alone, and in a third series vacuum-
mixed under pressure. Additionally, the ultimate static bending streng
th was investigated using the standard four-point bending test for the
three series of bone cement. Vacuum-mixing brought about an improveme
nt in the dynamic strength of Sulfix-60 from 6.3 MPa to 9.1 MPa, and f
or Allofix-G from 6.3 MPa to 8.2 MPa; additional pressure brought no f
urther improvement. A 200% increased fatigue stability was detectable
in comparison with the older cement. The ultimate bending strength was
also significantly improved by vacuum-mixing for both bone cements.