R. Nowak et al., SURFACE DEFORMATION OF SAPPHIRE CRYSTAL, Philosophical magazine. A. Physics of condensed matter. Structure, defects and mechanical properties, 74(1), 1996, pp. 171-194
The anisotropic surface deformation of sapphire has been studied by me
ans of depth-sensing indentation experiments with a small-radius spher
ical indenter loaded onto the basal (0001) and the prismatic (<10(1)ov
er bar 0>) planes of the crystal. The results of the low-speed high-ac
curacy continuous-indentation test have revealed significant differenc
es in the mechanical behaviour of alumina crystals when indented on di
fferent crystallographic planes. A special effort has been made to cla
rify the origin of the characteristic discontinuities appearing in the
loading part of the indentation hysteresis loops observed for the exp
eriments performed on the (0001) as well as (<10(1)over bar 0>) planes
of sapphire. It was concluded that the large 'step-in' reflects the f
ormation of a twin in g-alumina crystals deformed with a blunt indente
r. A new resolved shear stress model has been pro-posed in order to me
et the requirements of spherical indentation. The results of numerical
calculations predicted the deformation systems activated in the vicin
ity of spherical indentation. The prediction correlated with the obser
vations of residual impressions.