M. Ashizuka et E. Ishida, CRACK CONFIGURATION BENEATH VICKERS INDENTATION IN Y2O3-CONTAINING TETRAGONAL ZIRCONIA POLYCRYSTALS, Nippon Seramikkusu Kyokai gakujutsu ronbunshi, 104(7), 1996, pp. 673-676
Crack configurations beneath Vickers indentations in 3 mol% Y2O3-conta
ining tetragonal zirconia polycrystals (Y-TZP) with grain sizes of 0.4
mu m (Z3Y-I) and 1.0 mu m (Z3Y-II) were measured using a stepwise pol
ishing technique. The crack configuration beneath the Vickers indentat
ion in Y-TZP was Palmquist type. The depth of the crack beneath the Vi
ckers indentation in Z3Y-II was smaller than that of the crack in Z3Y-
I. Upheaval was observed around Vickers and Knoop indentations, and on
both sides of induced cracks. The height of the upheaval was about 2
mu m around the corner and the edge of the Vickers indentation. Howeve
r, the height of the upheaval around the induced crack decreased progr
essively away from the indentation. The upheaval had a maximum value o
f about 2 mu m at the end of the minor axis in the Knoop indentation.
However, the upheaval at the edge decreased linearly away from the min
or axis and was zero at the end of the apse axis. No crack was induced
beneath the Knoop indentation even if Y-TZP was indented using a load
of 490 N.