THE X-RAY-FLUORESCENCE MEASUREMENT PLACE AT BEAMLINE-L OF HASYLAB

Citation
F. Lechtenberg et al., THE X-RAY-FLUORESCENCE MEASUREMENT PLACE AT BEAMLINE-L OF HASYLAB, Journal of trace and microprobe techniques, 14(3), 1996, pp. 561-587
Citations number
64
Categorie Soggetti
Chemistry Analytical
ISSN journal
07334680
Volume
14
Issue
3
Year of publication
1996
Pages
561 - 587
Database
ISI
SICI code
0733-4680(1996)14:3<561:TXMPAB>2.0.ZU;2-3
Abstract
The following article describes the experimental facility for synchrot ron radiation induced X-ray fluorescence analysis (SYXRF) at beamline L of the Hamburger synchrotron radiation laboratory (Hasylab) at the D eutsches Elektronen-Synchrotron (DESY) in Hamburg. At the facility sim ple bulk analysis (SYXRF), high spatial resoluting measurements (mu-SY XRF), total reflection experiments (TR-SYXRF), surface analysis by mea ns of grazing incidence (SY-GIXA) and analysis of crystallographic par ameters by means of Kossel diffraction are possible. A great variety o f excitation spectra can be chosen by absorbers, reflectors and a mono chromator. The beam size is defined either by cross slits or by a focu sing capillary. The measurements take place in air or helium atmospher e, and the fluorescence radiation is detected by either a Si(Li) or HP Ge detector depending on the energy range of interest. The major advan tages are an easy to handle control of the highly flexible setup, smal l beam sizes, and low detection limits.