A FACILE ACCESS TO NUCLEOSIDE PHOSPHOROFLUORIDATE, NUCLEOSIDE PHOSPHOROFLUORIDOTHIOATE, AND NUCLEOSIDE PHOSPHOROFLUORIDODITHIOATE MONOESTERS

Authors
BOLLMARK M STAWINSKI J
Citation
M. Bollmark et J. Stawinski, A FACILE ACCESS TO NUCLEOSIDE PHOSPHOROFLUORIDATE, NUCLEOSIDE PHOSPHOROFLUORIDOTHIOATE, AND NUCLEOSIDE PHOSPHOROFLUORIDODITHIOATE MONOESTERS, Tetrahedron letters, 37(32), 1996, pp. 5739-5742
Citations number
22
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Tetrahedron letters → ACNP
ISSN journal
00404039
Volume
37
Issue
32
Year of publication
1996
Pages
5739 - 5742
Database
ISI
SICI code
0040-4039(1996)37:32<5739:AFATNP>2.0.ZU;2-T
Abstract
Oxidation of H-phosphonate, H-phosphonothioate, or H-phosphonodithioat e monoesters with iodine in pyridine in the presence of trimethylsilyl chloride, followed by addition of triethylamine trishydrofluoride (TA F) furnished rapid and quantitative formation of the corresponding pho sphorofluoridate, phosphorofluoridothioate, or phosphorofluoridodithio ate monoesters. Copyright (C) 1996 Elsevier Science Ltd.