J. Martinezfernandez et al., FERROELASTICITY OF THE DISPLACIVE TETRAGONAL PHASE IN Y2O3 PARTIALLY-STABILIZED ZRO2 (Y-PSZ) SINGLE-CRYSTALS, Journal of materials research, 11(8), 1996, pp. 1972-1978
Ferroelasticity of the tetragonal displacive (t') phase was studied on
4.7 mol% Y2O3 partially stabilized zirconia single crystals. Samples
were deformed at 1400 degrees C at constant strain rate to induce the
ferroelastic behavior. Domain reorientation due to the applied stress
has been studied as a function of the compression axis and aging time
at 1600 degrees C. Domain switching was found in the as-received and 2
-h-aged crystals deformed along the [100] direction, in which an excep
tional high flow stress was reached (>700 MPa). Transmission electron
microscopy observations were performed on deformed and undeformed crys
tals to study the microstructural changes associated with the domain s
witching. Incremental strain steps on the stress-strain curves and sur
face texture on the lateral faces of the deformed samples were correla
ted with the microstructural evidence.