D. Billaud et al., STRUCTURAL CHARACTERIZATION OF SELECTED M(X)C(60) PHASES (M=LI,NA,K) SYNTHESIZED ELECTROCHEMICALLY IN ALL-SOLID-STATE CELLS, Fullerene science and technology, 4(6), 1996, pp. 1119-1154
Electroreduction of C-60 was carried out in all-solid-cells operating
with polymer electrolytes composed of polyethylene oxide (PEG), and sa
lts like LiClO4, NaCF3SO3 or KCF3SO3. Some selected reduced phases of
C-60 were isolated and characterized by electron diffraction microscop
y.