SYNTHESIS OF 1,2-BIS(METHOXYAMINO)CYCLOALKANES FROM ALICYCLIC 1,2-BIS(HYDROXYAMINES)

Authors
MAZHUKIN DG KHLESTKIN VK TIKHONOV AY VOLODARSKY LB
Citation
Dg. Mazhukin et al., SYNTHESIS OF 1,2-BIS(METHOXYAMINO)CYCLOALKANES FROM ALICYCLIC 1,2-BIS(HYDROXYAMINES), Russian chemical bulletin, 45(4), 1996, pp. 880-884
Citations number
8
Categorie Soggetti
Chemistry
Journal title
Russian chemical bulletin → ACNP
ISSN journal
10665285
Volume
45
Issue
4
Year of publication
1996
Pages
880 - 884
Database
ISI
SICI code
1066-5285(1996)45:4<880:SO1FA1>2.0.ZU;2-N
Abstract
Derivatives of 1,4-dihydroxypiperazine-2,3-dione were obtained by reac tion of cis-1,2-bis(hydroxyamino)cycloalkanes with diethyl oxalate. Th eir alkylation with CH2N2 or Mel afforded 1,4-dimethoxypiperazine-2,3- diones. Hydrolysis of the latter gave 1,2-bis(methoxyamino)cycloalkane s.