MULLITE FABRICATION FROM FUMED SILICA AND BOEHMITE SOL PRECURSORS

Citation
Ar. Boccaccini et al., MULLITE FABRICATION FROM FUMED SILICA AND BOEHMITE SOL PRECURSORS, Materials letters, 29(1-3), 1996, pp. 171-176
Citations number
33
Categorie Soggetti
Material Science","Physics, Applied
Journal title
ISSN journal
0167577X
Volume
29
Issue
1-3
Year of publication
1996
Pages
171 - 176
Database
ISI
SICI code
0167-577X(1996)29:1-3<171:MFFFSA>2.0.ZU;2-D
Abstract
A particular combination of commercially available silica and alumina precursors (fumed silica nanopowders and a boehmite sol) have been use d to prepare mullite ceramics using colloidal processing and transient viscous sintering. The simple pressureless sintering route employed p roduced dense monolithic mullite samples at temperatures much lower th an those used in other studies. A very homogeneous and fine microstruc ture (grain size approximate to 0.8 mu m) was achieved by firing cold- isostatically pressed ''green'' compacts for 2 h at 1200 degrees C fol lowed by 5 h at 1350 degrees C.