This investigation is aimed at diagnostic studies on the behavior at d
ifferent interfaces in fiber reinforced concrete: between hardened cem
ent paste and sand, between mortar and coarse aggregate and between co
ncrete and fibers. Other types of internal failure include aggregate c
rushing, fiber rupture, and so on. Only cylindrical specimens, with va
rying volume percentage and aspect ratio of fibers, have been tested i
n compression. For quite some time additives like latexes, plasticizer
s, fibers and silica fume are incorporated in concrete and mortar to i
mprove one quality or the other of concrete, but one single common obj
ective is delaying or arresting interface cracks. This investigation a
ttempts to relate external behavior to internal signals of distress th
rough acoustic emission. This helps to identify critical internal dist
ress vis-a-vis external level of stress. Further, spectral analysis of
acoustic signals has been attempted in frequency domain in order to e
stablish which types of interface failure are predominant at different
stages of stress. Such understanding could enable material scientists
to decide on the parameters of additives with greater confidence when
developing composites with desired external response. Of interest are
instrumentation and on-line data processing in order to record (a) cu
mulative acoustic activity and (b) spectral analysis in frequency doma
in at different stages of progressive loading.