SYNTHESIS OF BENZOTRIAZOLO[1,2-ALPHA]BENZOTRIAZOLE DERIVATIVES AS NEWHIGH-DENSITY, INSENSITIVE ENERGETIC MATERIALS

Citation
G. Subramanian et al., SYNTHESIS OF BENZOTRIAZOLO[1,2-ALPHA]BENZOTRIAZOLE DERIVATIVES AS NEWHIGH-DENSITY, INSENSITIVE ENERGETIC MATERIALS, Journal of organic chemistry, 61(17), 1996, pp. 5801-5803
Citations number
16
Categorie Soggetti
Chemistry Inorganic & Nuclear
ISSN journal
00223263
Volume
61
Issue
17
Year of publication
1996
Pages
5801 - 5803
Database
ISI
SICI code
0022-3263(1996)61:17<5801:SOBDAN>2.0.ZU;2-7
Abstract
The synthesis of the new high density energetic compound [3',4':4,5]be nzotriazolo[1,2-a]benzotriazol-13-ium inner salt 1,11-dioxide (7) was achieved in three steps (37% yield) from -tetranitrobenzotriazolo[1,2- a]benzotriazolo-6-ium inner salt(4). The compound 7 was found to be th ermally stable up to 274 degrees C and was insensitive to impact (hamm er/anvil test).