The method is based on measuring the neutron cross-section of a powder
ed sample at neutron wavelengths beyond its Bragg cutoff. The effect o
f the neutron beam broadening due to its transmission through the powd
er sample on cross-section was treated as small angle neutron scatteri
ng (SANS) cross-section. The SANS cross-section was determined as the
difference between its measured cross-section in powder form and in bu
lk metal. At certain conditions the SANS cross-section values of powde
red samples were found to be inversely proportional to the particle si
ze. The method was applied for particle size determination of iron pow
ders. The accuracy in particle size was found to be 8%.