Dm. Grant et al., BIOCOMPATIBLE AND MECHANICAL-PROPERTIES OF LOW-TEMPERATURE DEPOSITED QUATERNARY (TI,AL,V)N COATINGS ON TI6AL4V TITANIUM-ALLOY SUBSTRATES, Journal of materials science. Materials in medicine, 7(9), 1996, pp. 579-584
A series of quaternary (Ti, Al, V) N coating layers were obtained by l
ow temperature reactive plasma sputtering in differing deposition cond
itions to improve the wear resistance and the biocompatibility of a ti
tanium surgical alloy, specifically Ti-6Al-4V. Characterization of the
mechanical properties, structure and the chemical composition of the
coating layer was explored by microhardness test, ball against flat we
ar test, scanning electron microscopy and X-ray diffraction. The bioco
mpatibility of the optimum coating layer (as determined by mechanical
performance) was examined by a modified MTT toxicity test and by monit
oring cell growth assessed by quantitative stereological analysis. The
experimental results are encouraging, indicating that this low temper
ature deposited, dense, quaternary (Ti,Al,V) N coating layer exhibits
improved mechanical properties such as high hardness and excellent adh
esion to a Ti alloy substrate and is highly biocompatible.