A VACUUM CHAMBER FOR LOW-BACKGROUND DIFFRACTION EXPERIMENTS

Citation
Rb. Neder et al., A VACUUM CHAMBER FOR LOW-BACKGROUND DIFFRACTION EXPERIMENTS, Zeitschrift fur Kristallographie, 211(9), 1996, pp. 591-593
Citations number
5
Categorie Soggetti
Crystallography
ISSN journal
00442968
Volume
211
Issue
9
Year of publication
1996
Pages
591 - 593
Database
ISI
SICI code
0044-2968(1996)211:9<591:AVCFLD>2.0.ZU;2-C
Abstract
We developed a small vacuum chamber for very low background single cry stal diffraction experiments. The chamber has been designed for a larg e Eulerian cradle. The phi and chi rotations are not limited by the ch amber, while the omega rotation is limited to a cone of 20 degrees ope ning angle. A crucial part of the design is the position of the beam s top inside the vacuum, eliminating any scattering at the exit windows. The chamber effectively eliminates any air scattering of the primary beam, creating a very low background for single crystal diffraction ex periments.