CRYSTAL-STRUCTURE OF OPHENYL)-5-METHYL-2,3-DIHYDRO-1H-PYRROLE-2,3-DIONE VERIFIES THE SCHEME OF SYNTHESIS

Authors
GROCHOWSKI J SERDA P DAUTER Z KOLASA A
Citation
J. Grochowski et al., CRYSTAL-STRUCTURE OF OPHENYL)-5-METHYL-2,3-DIHYDRO-1H-PYRROLE-2,3-DIONE VERIFIES THE SCHEME OF SYNTHESIS, Zeitschrift fur Kristallographie, 211(9), 1996, pp. 622-625
Citations number
15
Categorie Soggetti
Crystallography
Journal title
Zeitschrift fur Kristallographie → ACNP
ISSN journal
00442968
Volume
211
Issue
9
Year of publication
1996
Pages
622 - 625
Database
ISI
SICI code
0044-2968(1996)211:9<622:COO>2.0.ZU;2-B
Abstract
The structure of the title compound, crystallized from benzene, in the monoclinic system, space group P2(1)/c, with a = 9.032(3) Angstrom, b = 10.111(1) Angstrom, c = 14.625(1) Angstrom, beta = 121.3(1)degrees, Z = 4, has been solved from diffraction data collected on 2D imaging plate detector. This method allowed successful integration of non-unif orm reflection profiles with short exposure time. Structural results r evealed correct reaction path in the synthesis.