ANNYLMETHOXYMETHYL)-1,3-DIOXAN-5-YL]-ETHANEDIAMIDE

Authors
ROSS JN WARDELL JL LOW JN FERGUSON G
Citation
Jn. Ross et al., ANNYLMETHOXYMETHYL)-1,3-DIOXAN-5-YL]-ETHANEDIAMIDE, Acta crystallographica. Section C, Crystal structure communications, 52, 1996, pp. 1961-1963
Citations number
9
Categorie Soggetti
Crystallography
Journal title
Acta crystallographica. Section C, Crystal structure communications → ACNP
ISSN journal
01082701
Volume
52
Year of publication
1996
Part
8
Pages
1961 - 1963
Database
ISI
SICI code
0108-2701(1996)52:<1961:A>2.0.ZU;2-G
Abstract
The title compound, 3-dioxan-5-yl]ethanediamide(2-)}bis(triphenyltin), [Sn-2(C6H5)(6)(C26H3ON2O8)], was isolated from the products of the (t riphenylstannyl)methylation of a 1:1 mixture of stereoisomers of roxym ethyl-2-phenyl-1,3-dioxan-5-yl)ethanediamide. The molecule lies about an inversion centre and the unique Sn atom has distorted tetrahedral g eometry, with Sn-C-alkyl and Sn-C-aryl distances of 2.154 (2) and 2.13 8 (2)-2.147 (3) Angstrom, respectively, and C-Sn-C angles in the range 105.5 (1)-113.2 (1)degrees.