PROCEDURE FOR THE CATALYTIC DETERMINATION OF ALDEHYDES USING THIN-LAYER CHROMATOGRAPHY

Citation
Eb. Smirnova et al., PROCEDURE FOR THE CATALYTIC DETERMINATION OF ALDEHYDES USING THIN-LAYER CHROMATOGRAPHY, Journal of analytical chemistry, 51(9), 1996, pp. 903-905
Citations number
9
Categorie Soggetti
Chemistry Analytical
ISSN journal
10619348
Volume
51
Issue
9
Year of publication
1996
Pages
903 - 905
Database
ISI
SICI code
1061-9348(1996)51:9<903:PFTCDO>2.0.ZU;2-Q
Abstract
It is demonstrated that thin-layer chromatography with catalytic detec tion can be applied to the separation and detection of aldehydes in mi xtures. A procedure for determining formaldehyde (3-100 mu g), benzald ehyde (0.2-2 mg), and bromoacetaldehyde (15-100 mu g) in mixtures is d eveloped. A procedure for determining bromoacetaldehyde in the presenc e of a 100-fold excess of its acetal is proposed.