On. Grebneva et al., INDUCTIVELY-COUPLED PLASMA-ATOMIC EMISSION DETERMINATION OF 13 RARE-EARTH ELEMENTS AND YTTRIUM IN GEOLOGICAL SAMPLES AFTER MICROWAVE DECOMPOSITION, Journal of analytical chemistry, 51(9), 1996, pp. 927-930
A method has been developed for the direct group determination of rare
-earth elements and Y at a level of n x 10(-4)-n x 10(-6)% by inductiv
ely coupled plasma atomic emission spectrometry after the microwave de
composition of samples. The method is simple and convenient; the time
of decomposition is reduced by 80%. This method was used to analyze st
andard reference materials: KH limestone, ST-1A trap, and BM-1 basalt.
The obtained results were compared with certified values and the resu
lts of the determination of rare-earth elements after preconcentration
and shown to be highly repeatable.