APPLICATION OF THERMOLUMINESCENCE TO DETERMINE THE PRESENCE OF PRECURSOR OXIDES IN HIGH T-C CERAMIC SUPERCONDUCTORS

Citation
G. Burrafato et al., APPLICATION OF THERMOLUMINESCENCE TO DETERMINE THE PRESENCE OF PRECURSOR OXIDES IN HIGH T-C CERAMIC SUPERCONDUCTORS, Nuclear instruments & methods in physics research. Section B, Beam interactions with materials and atoms, 116(1-4), 1996, pp. 531-535
Citations number
15
Categorie Soggetti
Physics, Nuclear","Nuclear Sciences & Tecnology","Instument & Instrumentation
ISSN journal
0168583X
Volume
116
Issue
1-4
Year of publication
1996
Pages
531 - 535
Database
ISI
SICI code
0168-583X(1996)116:1-4<531:AOTTDT>2.0.ZU;2-K
Abstract
The thermally stimulated luminescence of oxides, carbonates and high T -c ceramic superconductors (perovskites of the (BiPb)SrCaCuO type obta ined by solid state reaction) was measured in the temperature interval 20-500 degrees C. The glow-curves obtained on the perovskites are com pared with those determined for both the precursor compounds and pure (BiPb)SrCaCuO powders of the same stoichiometry. The analysis of the d ata evidences the possibility of characterising the oxides and carbona tes and of detecting very low intensity TL signals produced in the sup erconductors by precursor compounds, which can be identified in some c ases, and/or low amounts of semiconducting or insulating compounds pro bably formed during the sintering procedure.