We report a development and application to SEM studies of semiconducto
rs of a cathodoluminescence spectrometer based on acoustooptical filte
rs, that has several advantages in comparison with commonly used spect
rometers and can be directly placed on a SEM electron-beam column. Dig
ital control and high transmission of the unit permit to measure spect
ra of cathodoluminescence emission of a solid solution of A(3)B(5) sem
iconductors and to study an image of the nonradiative defects in a mul
ti quantum well active layer of laser heterostructures. The results ar
e discussed on the point of view of initial stages of growth of an InP
layer on the surface of InGaAs layer during the MOCVD epitaxial growt
h of heterostructures.