ANISOTROPIC CRYSTALLINE GROWTH DEVELOPED IN BANGLADESHI COKING COAL DURING MESOPHASE TRANSFORMATION

Citation
J. Podder et T. Hossain, ANISOTROPIC CRYSTALLINE GROWTH DEVELOPED IN BANGLADESHI COKING COAL DURING MESOPHASE TRANSFORMATION, Thermochimica acta, 284(2), 1996, pp. 279-287
Citations number
14
Categorie Soggetti
Chemistry Analytical
Journal title
ISSN journal
00406031
Volume
284
Issue
2
Year of publication
1996
Pages
279 - 287
Database
ISI
SICI code
0040-6031(1996)284:2<279:ACGDIB>2.0.ZU;2-4
Abstract
The anisotropy of the mesophase spherules is developed during the carb onization of extracted coking coal in the temperature range 430 to 450 degrees C. Mesophase transition is observed by the differential scann ing calorimetric study. Enthalpy Delta H involved in the mesophase tra nsformation is found to be 46.26 J/g. The growth of mesophase spherule s, their coalesced structures, mosaic and flow type mosaic are observe d by the polarized light technique as the evidence of graphitizing car bon. The solvent extraction of coking coal is carried out using benzen e as a solvent at atmospheric pressure by Soxhlet apparatus.