Rb. Grishaber et al., EFFECT OF TESTING ENVIRONMENT ON INTERGRANULAR MICROSUPERPLASTICITY IN AN ALUMINUM MMC, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 220(1-2), 1996, pp. 78-84
A correlation between the testing environment and the observed high te
mperature deformation characteristics of a Al 6090 (Al-Mg-Si-Fe-Cu all
oy) + 25 vol.% SiCp metal matrix composite (MMC) has been conducted. P
ost deformation observations were performed on similar material specim
ens tested in uniaxial tension to failure within either air or argon h
igh temperature environments. Intragranular grain boundary whiskers th
at exhibited exceptionally high local superplastic-like elongations we
re observed when deformed in air at a temperature which was approximat
ely 80% of, or greater than, the incipient melting point of the matrix
and at a strain-rate of 4 x 10(-4) s(-1) whereas in a relatively pure
argon environment under similar deformation conditions, the whiskerin
g phenomenon (i.e. microsuperplastic whiskering, MSPW) at failure was
not observed. Differential thermal analysis of the MMC microstructure
verified that the observed MSPW behavior was a solid-state deformation
process rather than being related to the presence of a liquid or semi
-solid. The chemical constitution of the observed whiskers is thermody
namically most likely to be of a spinel compound, MgAl2O4.