SYNTHESIS OF MONOPHASE HGBA2CUO4-PRESSURE(DELTA UNDER CONTROLLED PARTIAL OXYGEN)

Authors
ALYOSHIN VA MIKHAILOVA DA ANTIPOV EV
Citation
Va. Alyoshin et al., SYNTHESIS OF MONOPHASE HGBA2CUO4-PRESSURE(DELTA UNDER CONTROLLED PARTIAL OXYGEN), Physica. C, Superconductivity, 255(3-4), 1995, pp. 173-179
Citations number
17
Categorie Soggetti
Physics, Applied
Journal title
Physica. C, Superconductivity → ACNP
ISSN journal
09214534
Volume
255
Issue
3-4
Year of publication
1995
Pages
173 - 179
Database
ISI
SICI code
0921-4534(1995)255:3-4<173:SOMHUC>2.0.ZU;2-G
Abstract
A reproducible method of synthesis of monophase HgBa2CuO4+delta is des cribed. The synthesis is carried out in sealed silica tubes under cont rolled partial oxygen pressure. The best results were obtained within the [0.012-0.15] bar partial oxygen pressure range at 800 degrees C. M ixtures of transition metal oxides, Co3O4/CoO or CuO/Cu2O, were used t o promote the exact regulation of the partial internal oxygen pressure .