J. Strempfer et al., THE NONRESONANT MAGNETIC-X-RAY SCATTERING CROSS-SECTION OF MNF2 .2. HIGH-ENERGY X-RAY-DIFFRACTION AT 80 KEV, Acta crystallographica. Section A, Foundations of crystallography, 52, 1996, pp. 438-449
Results of high-energy non-resonant magnetic X-ray diffraction experim
ents performed on the model system MnF2 at a photon energy of 80 keV a
re presented, A surprisingly high peak intensity of the magnetic 300 r
eflection of 13000 photons s(-1) in the three-crystal mode and 19000 p
hotons s(-1) in the two-crystal mode, with a peak-to-background ratio
of 230:1 and 10:1, respectively, has been achieved. At 80 keV, the pen
etration depth is 7 mm. When the path length of the beam through the c
rystal is varied, the effect of volume enhancement of the intensity di
ffracted by magnetic reflections is demonstrated. The Q dependence of
the magnetic and the charge Bragg reflections has been measured and ag
rees well with theory. The measurement of the temperature dependence o
f the sublattice magnetization allows a very accurate determination of
the critical exponent beta = 0.333 (3) and the Neel temperature T-N =
67.713 (2) K. Finally, the multiple charge scattering is discussed, w
hich is very pronounced for the magnetic reflections of MnF2.