Aa. Bolzan et al., A SPECTROSCOPIC COMPARISON OF YBCO SUPERCONDUCTORS SYNTHESIZED BY SOLID-STATE AND COPRECIPITATION METHODS, Materials letters, 28(1-3), 1996, pp. 27-32
Raman spectroscopy, X-ray diffraction (XRD), and scanning electron mic
roscopy (SEM) have been used to compare samples of YBa2Cu3O7 (YBCO) sy
nthesised by the solid-state method and a novel co-precipitation techn
ique. XRD results indicate that YBCO prepared by these two methods are
phase pure, however the Raman and SEM results show marked differences
between these samples.