SILICONE-COATED ALUMINA POWDERS BY THE EMULSION TECHNIQUE

Citation
Lj. Neergaard et al., SILICONE-COATED ALUMINA POWDERS BY THE EMULSION TECHNIQUE, Journal of Materials Science, 31(18), 1996, pp. 4779-4783
Citations number
11
Categorie Soggetti
Material Science
ISSN journal
00222461
Volume
31
Issue
18
Year of publication
1996
Pages
4779 - 4783
Database
ISI
SICI code
0022-2461(1996)31:18<4779:SAPBTE>2.0.ZU;2-X
Abstract
Alumina powders were prepared using an emulsion technique to chemicall y bond silanol-terminated poly dimethylsiloxane (PDMS or silicone) to the surface of alumina powders. Stable aqueous emulsions of silicone w ere prepared using Tween-80 surfactant. Transmission optical microscop y was used to measure the oil-droplet and coated-particle sizes. Fouri er transform-infrared spectroscopy was used to quantify bonding betwee n the silicone and the Al2O3. Coated powders were dry-pressed, and PDM S was compared to paraffin for dry-pressing behaviour and green streng th. Densification studies were made on powders. X-ray diffraction and scanning electron microscopy were used to characterize the sintered ce ramic.