OPTIMALLY INTERFACING AN ICP-MS WITH A CONVENTIONAL AUTOSAMPLER FOR THE ANALYSIS OF SOLUTIONS WITH A HIGH DISSOLVED SOLIDS CONTENT USING CONTINUOUS NEBULIZATION
Y. Gelinas et al., OPTIMALLY INTERFACING AN ICP-MS WITH A CONVENTIONAL AUTOSAMPLER FOR THE ANALYSIS OF SOLUTIONS WITH A HIGH DISSOLVED SOLIDS CONTENT USING CONTINUOUS NEBULIZATION, Atomic spectroscopy, 17(4), 1996, pp. 143-147
A simple interfacing method for the optimal coupling of the basic soft
ware of an ICP-MS with a conventional automatic sampler is described.
It is designed to facilitate the quantitative analysis of solutions wi
th a high dissolved solids content by eliminating the need for a signa
l stabilization time and by reducing the sample introduction system ri
nsing time. The general characteristics are presented along with the a
nalytical figures of merit. The main benefits of this method include a
n increased sample throughput (120 seconds per sample), a minimal amou
nt of material needed, and a reduced maintenance frequency of the samp
ler/skimmer cones and the nebulizer/desolvation chamber/torch assembly
. It thus represents a valuable alternative to the traditional choice
between conventional continuous nebulization and the purchase of a now
injection analysis system.