Jp. Chen et De. Nikles, PREPARATION OF ACICULAR ALPHA-FE NANOPARTICLES IN A LAMELLAR LIQUID-CRYSTALLINE PHASE, IEEE transactions on magnetics, 32(5), 1996, pp. 4478-4480
Acicular alpha-Fe nanoparticles were prepared by sodium borohydride re
duction of ferrous chloride in the presence of the liquid crystalline
system, C(12)EO(4)/water. The shape of the acicular particles was temp
lated by the colloid and a magnetic field. The acicular particles obta
ined from the lamellar phase were 50 similar to 150 nanometers long an
d 5 nanometers wide. The product also included some spherical particle
s of 10 similar to 15 nanometers in diameter. The saturation magnetiza
tion was 94 emu/g and the coercivity was 420 Oe.