A novel method using atomic force microscopy (AFM) to study optical fi
bre structures at the fibre end-face has been successfully developed.
The doping concentration profiles of fibres revealed by differential e
tching speeds in a saturated solution of ammonium bifluoride at room t
emperature (25 degrees C) were obtained from AFM topographic images. T
he superior spatial resolution of AFM made it possible to resolve conc
entric structures a hundred times smaller than the feature, due to the
difference in the known refractive index (Delta n) of 1 x 10(-3). Fib
res with small core diameters and anisotropic structures, such as pola
rization-maintaining fibres, were studied with ease.