Jw. Nicholson et F. Abiden, CHANGES IN COMPRESSIVE STRENGTH ON AGING IN GLASS POLYALKENOATE (GLASS-IONOMER) CEMENTS PREPARED FROM ACRYLIC MALEIC ACID COPOLYMERS/, Biomaterials, 18(1), 1997, pp. 59-62
Previous studies have shown that glass-ionomers made from acrylic/male
ic acid copolymers stored in water reach a maximum strength at about 1
week, and after 4 months have become significantly weaker. This findi
ng, which contrasts with the behaviour of glass-ionomers based on poly
(acrylic acid), was originally attributed to hydrolytic instability. T
his interpretation has been tested in the current work. Specimens of g
lass-ionomer prepared from acrylic/maleic acid copolymer have been sto
red for up to 4 months in different media, namely deionized water, dry
air and vegetable oil, then tested for compressive strength. Specimen
s were in the form of cylinders of dimensions 6 mm high x 4 mm diamete
r, and storage temperature was 37 degrees C. Data were analysed using
two-way analysis of variance (ANOVA) and in all three media specimens
became weaker at 4 months than they had been at 1 week (P < 0.05). How
ever, for the specimens stored in dry air and in water, the 1-week val
ues were not the maximum. The fact that there was a loss of strength u
nder all conditions led to the conclusion that it is not, after all, d
ue to hydrolysis. (C) 1996 Elsevier Science Limited