QUALITATIVE AND QUANTITATIVE-DETERMINATION OF 2,4,6-TNT, HEXOGEN, OCTOGEN, AMINONITROCOMPOUND AND NITROCOMPOUND IN AMMUNITION WASTES WITH MODIFIED TLC AND HPTLC PRECOATED LAYERS

Authors
KESSEL S HAUCK HE
Citation
S. Kessel et He. Hauck, QUALITATIVE AND QUANTITATIVE-DETERMINATION OF 2,4,6-TNT, HEXOGEN, OCTOGEN, AMINONITROCOMPOUND AND NITROCOMPOUND IN AMMUNITION WASTES WITH MODIFIED TLC AND HPTLC PRECOATED LAYERS, Chromatographia, 43(7-8), 1996, pp. 401-404
Citations number
6
Categorie Soggetti
Chemistry Analytical","Biochemical Research Methods
Journal title
Chromatographia → ACNP
ISSN journal
00095893
Volume
43
Issue
7-8
Year of publication
1996
Pages
401 - 404
Database
ISI
SICI code
0009-5893(1996)43:7-8<401:QAQO2H>2.0.ZU;2-O
Abstract
A thin layer chromatographic method for a qualitative screening-test a nd a quantitative analysis of 2,4,6-TNT, biodegradation products, octo gen and hexogen in ammunition wastes was developed using both polar an d non-polar modified sorbents. For enrichment a solid-phase extraction on LiChrolut(R) EN followed by removal with methanol/acetonitrile (1: 1 v/v) was chosen. To imitate real samples, spiked tap water samples o f known composition were used.