A. Higazy et al., RENDERING FLAX FIBER DYEABLE WITH BASIC-DYES VIA PARTIAL CARBOXYMETHYLATION, Journal of the Society of Dyers and Colourists, 112(11), 1996, pp. 329-332
Carboxymethylation of flax has been carried out by first treating the
fibres with sodium hydroxide followed by the sodium salt of monochloro
acetic acid. The treatment was carried out under a variety of conditio
ns. Variables studied included concentrations of monochloroacetic acid
and sodium hydroxide in the impregnating solutions, as well as durati
on and temperature of the reaction. It was found that the extent of ca
rboxymethylation increased substantially by controlling the concentrat
ions of alkali and monochloroacetic acid, and by reacting for 60 min a
t 70 degrees C. The behaviour of selected samples of partially carboxy
methylated flax towards basic dyes was also studied.