Ak. Gupta et al., REVIEW OF THE TECHNIQUES FOR THE EXTRACTION OF 2ND-PHASE PARTICLES FROM ALUMINUM-ALLOYS, Materials characterization, 37(2-3), 1996, pp. 61-80
This article briefly reviews the methods developed for extracting the
second-phase particles from aluminum alloys. The chemical phenol extra
ction technique has been compared with the electrochemical potassium i
odide (KI)-in-methanol method for two heat-treatable 6000-series alloy
s. It is demonstrated that by carrying out the centrifuging warm in th
e phenol method, the technique can handle quite large sample sizes wit
hout contamination and regardless of the heat-treated condition of the
sample under examination. In contrast, the KI-in-methanol method is l
imited to homogenized materials. The phenol particle extraction from h
igh-Cu (<1.0%)-containing alloy showed contamination arising from the
metallic Cu that appears to originate from the Cu in the matrix, rathe
r than from Cu-containing second-phase-particles. (C) Elsevier Science
Inc., 1996