L. Kloc et al., SIGNIFICANCE OF CONTINUOUS PRECIPITATION DURING CREEP OF A POWDER-METALLURGY ALUMINUM-ALLOY, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 216(1-2), 1996, pp. 161-168
Experiments were conducted to evaluate the creep properties of a 2024
aluminum alloy fabricated by powder metallurgy processing. The creep c
urves exhibit a minimum creep rate followed by an extended tertiary st
age prior to failure. Using the values of the minimum creep rates, the
apparent stress exponents are high and variable suggesting the presen
ce of a threshold stress. Observations using transmission electron mic
roscopy (TEM) reveal the occurrence of a continuous precipitation of f
ine particles during the tests. Although the density of these particle
s is dependent upon the testing conditions, quantitative measurements
show that their average size is of the order of similar to 60 nm under
all conditions. A temperature compensated time is introduced to descr
ibe the evolution of fine particles during testing, and this permits t
he development of a relationship which can be used to estimate the den
sity of fine particles under any selected conditions.