Sk. Wu et al., A STUDY ON THE WIRE DRAWING OF TINI SHAPE-MEMORY ALLOYS, Materials science & engineering. A, Structural materials: properties, microstructure and processing, 215(1-2), 1996, pp. 113-119
Drawn wires of TiNi shape memory alloys (SMAs) have been studied syste
matically using DSC, microhardness, SEM and tensile tests. Severe work
hardening during the drawing process is observed and hence interannea
ling is necessary. Multi-pass drawing around the Ms temperature is rec
ommended. The defects induced by cold drawing depress martensitic tran
sformation but promote the R-phase transformation. Defect recovery and
recrystallization during interannealing are responsible for the decre
ase of drawing stress. At the same time, surface oxide film thickness
is another important factor related to drawing stress. A thin surface
oxide film can be used as a lubricant during the drawing process, howe
ver, thick oxide films tend to exhibit cracks and spalling which decre
ase the drawing surface quality, shape memory effect and pseudoelastic
ity of TiNi SMAs. MoS2 is shown to be an effective lubricant for the w
ire drawing of TiNi SMAs.