Multilayer materials appears today very studied in order to increase t
hese physico-chemical characteristics. The determination of residual s
tresses that occur during the elaboration of multilayers is very impor
tant in the knowledge of these properties but also the metal/metal int
erfaces one. This study uas made on Au/Ni multilayers obtained by mole
cular beam epitaxy. Residual stress were determined by X-ray diffracti
on using triaxial analysis of stresses and ''sin(2) psi'' method.