F. Bridou et B. Pardo, USE OF THE FOURIER SPECTRUM OF X-RAY REFL ECTIVITY CURVES FOR ANALYSIS OF STACKED THIN-LAYERS, Journal de physique. IV, 6(C4), 1996, pp. 367-383
Grazing incidence X-my reflectometry is usually used for the analysis
of thin layer stacks. The parameters to be found are thicknesses, roug
hnesses, and indices. They can be reached by the fitting of the experi
mental reflectivity curve whith a theoretical one calculated from thes
e parameters (trial and error method). Another method consists to use
the Fourier transform in order to study the typical features of the st
ack. Because the reflectivity curve has no periodicity, the data have
to be processed before using the Fourier transformation.Starting from
real examples, it will be shown how the Fourier analysis gives informa
tions on the model of the stack The results allows mainly to evaluate
the distances between all the interfaces. The accuracy of the results
depends on the angular detection scanning range. The width of the peak
s in the spectrum depends on the roughness of the related interfaces.
A limitation of this method is due to the discretisation of the Fourie
r transform. The results are refined by the trial and error method as
explained above, but with starting roughtly known values of the parame
ters, that allows to save much time in the curves fitting process.