Yi. Korenman et al., 2-STAGE PRECONCENTRATION AND GAS-CHROMATOGRAPHIC DETERMINATION OF PHENOLS IN NATURAL-WATERS, Journal of analytical chemistry, 51(11), 1996, pp. 1038-1040
In order to develop a gas chromatographic method for determination of
phenols in natural waters, some regularities of the distribution of ph
enols between organic solvents of different classes and an aqueous sal
ine solution are studied. The best conditions for eliminating petroleu
m products from the concentrate are found. The losses in volatile phen
ols due to preconcentration are insignificant and do not cause any inc
rease in the relative error of determination by the internal-standard
method. The results of determinations of phenols in amounts close to t
heir maximum permissible concentrations (MPC) are given.