Wz. Wu et al., COMPARATIVE EXTRACTION OF POLYCHLORINATED DIBENZO-P-DIOXINS AND DIBENZOFURANS (PCDD F-S) FROM A VARIETY OF SOLID SAMPLES/, Chemosphere, 33(11), 1996, pp. 2229-2237
Extraction experiments with spiking of C-13(12)-PCDD/Fs were performed
with a variety of PCDD/Fs contaminated samples. The extraction recove
ry of PCDD/Fs was mainly influenced by PCDD/Fs concentration and the s
ample matrix. Generally, the first soxhlet extraction with toluene has
suitable recovery. From the selected samples, only FAMS4 and 5 which
are fly ashes with high concentration, the recovery of the first soxhl
et extraction with 24 hr. is low, but PCDD/Fs were almost completely r
emoved after 72 hr. Copyright (C) 1996 Elsevier Science Ltd