PREPARATION AND CHARACTERIZATION OF NEW C-SULFONYLDITHIOFORMATES AND THEIR THIOCARBONYL S-IMIDES

Authors
ELSAYED I ABDELMEGEED MF YASSIN SM SENNING A
Citation
I. Elsayed et al., PREPARATION AND CHARACTERIZATION OF NEW C-SULFONYLDITHIOFORMATES AND THEIR THIOCARBONYL S-IMIDES, Phosphorus, sulfur and silicon and the related elements, 86(1-4), 1994, pp. 239-257
Citations number
51
Categorie Soggetti
Chemistry Inorganic & Nuclear
Journal title
Phosphorus, sulfur and silicon and the related elements → ACNP
ISSN journal
10426507
Volume
86
Issue
1-4
Year of publication
1994
Pages
239 - 257
Database
ISI
SICI code
1042-6507(1994)86:1-4<239:PACONC>2.0.ZU;2-Y
Abstract
Two new chlorodithioformates 2, six new C-sulfonyldithioformates 3, te n new chloromethanesulfenyl chlorides 4, and nineteen new C-sulfonyldi thioformate S-imides 5 have been prepared. Together with analogous kno wn compounds they were fully characterized by spectroscopic means (IR, UV/VIS, MS, C-1 and C-13 NMR). According to these data and additional X-ray crystallographic structure determinations of selected 5 all kno wn 5 possess the (E)-configuration and no evidence for the presence of isomeric (Z)-5 could be found.