CRYSTAL-STRUCTURE OF THE PRODUCT FROM ACID-CATALYZED DIMERIZATION OF THE INTERMEDIATE FORMED DURING HYDROGENOLYSIS OF 2-(BENZO[B]THIOPHEN-2-YL)PROPAN-2-OL

Authors
BANERJEE A BISWAS G BISWAS SP MAJI BB GHATAK KL GANGULY SN LITAKA Y
Citation
A. Banerjee et al., CRYSTAL-STRUCTURE OF THE PRODUCT FROM ACID-CATALYZED DIMERIZATION OF THE INTERMEDIATE FORMED DURING HYDROGENOLYSIS OF 2-(BENZO[B]THIOPHEN-2-YL)PROPAN-2-OL, Journal of chemical research. Synopses, (2), 1995, pp. 60-61
Citations number
9
Categorie Soggetti
Chemistry
Journal title
Journal of chemical research. Synopses → ACNP
ISSN journal
03082342
Issue
2
Year of publication
1995
Pages
60 - 61
Database
ISI
SICI code
0308-2342(1995):2<60:COTPFA>2.0.ZU;2-Q
Abstract
The hydrogenolysis of 2-(benzo[b]thiopen-2-yl)propan-2-ol with triethy lsilane and trifluoroacetic acid not only afforded the expected 2-isop ropylbenzo[b]thiophene (1) but also a dimeric benzo[b]thiophene deriva tive (4) as a racemic mixture, the structure of which was confirmed by X-ray analysis.