Elastic neutron diffraction experiments on amorphous iron, cobalt and
their amorphous binary metallic alloys are presented. The measurements
allow, and for the first time, to describe the atomic distribution in
samples obtained in the form of fine (<30 nm) amorphous elemental par
ticles by sonochemical synthesis. In the case of a-Fe, the structural
information from the shape of the radial distribution function is cons
istent with the Random Packing model (RPD) calculations previously mad
e for films of amorphous iron. Finally the atomic magnetic moment of i
ron and cobalt in the amorphous bulk phase is also evaluated.