E. Yanmaz et al., AG-DOPED 120-K YBA2CU3O7-DELTA SUPERCONDUCTORS PREPARED BY THE FLAME-QUENCH-MELT-GROWTH (FQMG) METHOD, Superconductor science and technology, 7(12), 1994, pp. 903-907
The effect of Ag-doping on the microstructure and physical properties
of YBa2Cu3O7-delta superconductors prepared by a flame-quench-melt-gro
wth (FQMG) process, was investigated. Pellets of YBa2Cu3O7-delta conta
ining 0-30 weight percentage (wt.%) of Ag were quenched by LPG-O-2 fla
me melting and then crushed to obtain powder which was compacted and t
hen subjected to a melt-growth process. As a result of this process, l
arge grained, textured YBCO material was produced. It was found that Y
BCO samples with 10 wt.% Ag doped showed a transition temperature of 1
20 K and further increasing the Ag content caused a decrease of transi
tion temperature. Using this modified quench-melt-growth technique, th
e reaction between crucibles and material can be completely avoided du
ring the preparation of the precursor materials.