Fk. Urban et al., MODELING OF SURFACE-ROUGHNESS IN VARIABLE-ANGLE SPECTROSCOPIC ELLIPSOMETRY, USING NUMERICAL PROCESSING OF ATOMIC-FORCE MICROSCOPY IMAGES, Thin solid films, 253(1-2), 1994, pp. 326-332
Variable-angle spectroscopic ellipsometry is used for ex situ investig
ation of thin films deposited on substrates. Calculation of the thickn
ess and optical properties of a number of films in a multilayer stack
is possible, because a large amount of data is taken over a wide range
of wavelengths and incidence angles. However, the authors here confir
m that significant surface roughness of the outermost film must be tak
en into acount for useful solutions. In our earlier work, the roughnes
s was modelled as a single roughness layer at the film ambient interfa
ce. This layer was taken to be an effective medium, composed of film a
nd voids. The thickness and void fraction were determined from atomic
force microscopy (AFM) measurements. Improvement in ellipsometry solut
ions has been achieved using a new model of the roughness layer compos
ed of six effective medium sublayers. Numerical processing of AFM data
is described, considering suface scans ranging from 1 mu m x 1 mu m t
o 12 mu m x 12 mu m. The complete deposited film was best modelled as
a rough surface layer (70 nm thick) over a continuous layer 350 nm thi
ck.