Jm. Letoffe et al., EVALUATION OF CRYSTALLIZED FRACTIONS OF CRUDE OILS BY DIFFERENTIAL SCANNING CALORIMETRY - CORRELATION WITH GAS-CHROMATOGRAPHY, Fuel, 74(1), 1995, pp. 92-95
Using differential scanning calorimetry (d.s.c.) apparatus, an experim
ental procedure has been developed in order to determine the wax conte
nt of 29 crude oils from several sources. The amount of wax, which is
obtained with good reproducibility, is higher than the values obtained
by gas chromatography (g.c.). In fact, g.c. evaluates n-alkanes and d
.s.c. evaluates the total amount of crystallized species (n-alkanes is
oalkanes, cycloalkanes,...,). The tested method is rapid, each run is
performed within 1 h.