Fluorinated dibenzo-p-dioxins (PFDD) have been selectively synthesized
from fluorophenols and isolated by liquid-column- and thin layer chro
matography. The structures were confirmed by IR, MS, HR-MS, H-1-NMR an
d F-19-NMR-spectroscopy. Reaction times, melting points and the IR-abs
orption bands are presented for several PFDD's as well as H-1- and (19
)-F-NMR-spectra for two PFDD's and the mass-spectrum for 2,3,7,8-T4FDD
.