The new norcucurbitacin glycosides, andirobicin A gentiobioside [2], a
nd andirobicin C gentiobioside [1], and the known fevicordin F gentiob
ioside [3], were isolated from the aqueous MeOH fraction of a liquid-l
iquid partition of the MeOH extract of the seeds of Fevillea trilobata
. Their structures were determined by nmr and ms techniques.