The applicability and usefulness of k(0)-based reactor neutron activat
ion analysis (NAA) in the life sciences is evaluated from the followin
g examples: 1. Instrumental NAA of NIST SRM 1633a coal fly ash, as a q
uality assessment; 2. Radiochemical NAA of Versieck's reference human
serum, and-herewith associated-the development of practical correction
procedures for neutron-induced reaction interferences and of improved
methods to evaluate the detection efficiency and the correction for t
rue coincidence; and 3. Determination of the lanthanides in plant leav
es and lichens near a Portuguese coal-fired power station, which led t
o the introduction of the Westcott formalism and to the use of a low-e
nergy photon detector. As concluded, k(0)-based NAA is at present capa
ble of tackling a large variety of analytical problems when it comes t
o the multielement determination in environmental and biological matri
ces.