The absorption of 150 keV synchrotron radiation in matter is weak and,
as normally done with neutrons, bulk properties are studied in large
samples. However, the k-space resolution obtained with a Triple Crysta
l Diffractometer (TCD) for high energy synchrotron radiation is about
one order of magnitude better than in high resolution neutron diffract
ion. The technique has been applied to measure the structure factor S(
Q) of amorphous solids up to momentum transfers of the order of 32 Ang
strom(-1), to study the intermediate range Ortho-II ordering in large,
high quality YBa2Cu3O6.5 single crystals and for investigations of th
e defect scattering from annealed Czochralski grown silicon crystals.
Magnetic superlattice reflections have been measured in MnF2 demonstra
ting the potential of the technique for high resolution studies of gro
und state bulk antiferromagnetism. Recently the question of two length
scales in the critical scattering at the 100 K phase transition in Sr
TiO3 was studied. At the PETRA storage ring, which serves as an accumu
lator for the HERA electron-proton-ring at DESY and which can be opera
ted up to electron energies of 12 GeV, an undulator beam line is curre
ntly under construction and should be available in summer 1995. It ope
ns up exciting new research opportunities for photon energies from abo
ut 20 to 150 keV.